制备工艺因素对碳化硅水基浆料粘度的影响研究
Research on Influence of Preparation Process on Viscosity of SiC Aqueous Slurry
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摘要: 研究了浆料搅拌时间、分散剂含量、粉体含量和pH值等对碳化硅水基浆料粘度的影响。结果表明,水基浆料的粘度随搅拌时间的增加而减小,超过24 h后趋于平稳;水基浆料粘度随分散剂含量的增加而减小,但超过一定含量时反而增大;随着SiC水基浆料中粉体含量的逐渐增加,浆料的粘度总体呈逐渐增大的趋势,粉体含量超过30%时,浆料的搅拌分散时间会延长1.5倍;p H值高于5.5后,水基浆料的粘度随p H值的增加急剧提高,超过8.15时略有下降。通过优化工艺参数,可制备出粘度低于1.0 Pa·s、粉体含量为30%的Si C水基浆料。Abstract: The influence of preparation processes such as stirring time of slurry,dispersant content,solids loading and p H value on viscosity of Si C aqueous paste were investigated. The results show that the slurry viscosity decreases with increasing stirring time and levels off when the stirring time exceeds 24 hours; the slurry viscosity decreases with increasing dispersant content but increases when the dispersant content exceeds a certain quantity; when the solid loading is higher than 30%,the slurry viscosity increases sharply and doesn't decrease even if the dispersant content is increased; when the p H value is above5. 5,the slurry viscosity increases rapidly with increasing p H value and slightly declines when the p H value exceeds 8. 15. By optimizing the preparation processes,the Si C aqueous slurry with viscosity of about 1. 0 Pa·s and 30% solid loading could be prepared.