Abstract: Due to the complexation charateristic and the active thiol of AMT, we adopted chloroacetic acid to modify the surface of boehmite to prepare anti-rust nano fillers, and then. the modified boemhite and epoxy resin were blend together to obtain anticorrosive coating under the high-speed dispersion condition. The on-line infrared method was chosen to analysis the release of the modified boehmite. At last, and the corrosion inhibition performance of modified boehmite was explored by electrochemical impedance spectroscopy method.Results revealed that the modified boehmite could release corrosive inhibitor, and evidently improve the anticorrosion performance of the coating.