DZ125定向凝固高温合金在温度-应力双场耦合作用下的组织演变与力学行为

Microstructure Evolution and Mechanical Behavior of DZ125 Directionally Solidified Superalloy under the Coupling Effect of Temperature-Stress Dual Fields

  • 摘要: 通过测试DZ125合金在900 ℃/250 MPa、950 ℃/250 MPa和980 ℃/250 MPa条件下的蠕变曲线,分析蠕变曲线特征,并测试其微观组织和显微硬度,研究温度对合金蠕变行为的影响。结果表明,随着蠕变温度从900 ℃提高980 ℃,蠕变断裂时间从246.00 h缩短到7.75 h,稳态蠕变速率由0.004 5%/h增加到0.224 4%/h;裂纹主要起源于表面的再结晶晶界和内部碳化物处,在温度、应力和氧化的共同作用下,部分表面再结晶晶粒从表面脱离;蠕变初期微观组织中的γ'相出现了垂直于应力方向的N型筏排化,蠕变后期筏排化γ'相发生扭曲断裂,蠕变时间越长扭曲越严重,其通道宽度越宽;蠕变试样的显微硬度一般低于原始试样,但高温短时断裂试样因组织中的γ'相处于初始筏排化阶段,其硬度反而有所升高;若DZ125合金零件承受应力约为250 MPa,该处的服役温度不宜超过980 ℃。

     

    Abstract: By testing the creep curves of DZ125 alloy under the conditions of 900 ℃/250 MPa, 950 ℃/250 MPa and 980 ℃/250 MPa and analyzing characteristics of the creep curves, testing its microstructure and microhardness, the influence of temperature on the alloy creep behavior was systematically studied. The results showed that as the creep temperature increased from 900 ℃ to 980 ℃, the creep rupture time shortened from 246.00 h to 7.75 h, and the steady-state creep rate increased from 0.004 5%/h to 0.224 4%/h. Cracks mainly originated from the recrystallized grain boundaries on surface and internal carbides, and under the combined action of temperature, stress and oxides, some surface recrystallized grains might detach from the surface. In the early stage of creep, the γ' phase in the microstructure might undergo N-type rafting perpendicular to the stress direction. In the later stage of creep, the rafted γ' phase experienced distortion and fracture. The longer the creep time, the more severe the distortion and the wider the channel width. Microhardness of the creep specimen was generally lower than that of the original specimen. However, for the specimen fractured at high temperature in a short time, its hardness actually increased due to the γ' phase being in the initial rafting stage. Therefore, when the stress on DZ125 alloy parts is approximately 250 MPa, the service temperature should not exceed 980 ℃.

     

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