PAN Yang, WEI Ya-bing, CHEN Hong-ling, SHI Shu-zhe. Synthetic Method and Surface-active Property of C8F17SO2N(C2H5)C2H4(OC2H4)nOH[J]. Development and Application of Materials, 2004, 19(3): 16-18,24. DOI: 10.19515/j.cnki.1003-1545.2004.03.005
Citation: PAN Yang, WEI Ya-bing, CHEN Hong-ling, SHI Shu-zhe. Synthetic Method and Surface-active Property of C8F17SO2N(C2H5)C2H4(OC2H4)nOH[J]. Development and Application of Materials, 2004, 19(3): 16-18,24. DOI: 10.19515/j.cnki.1003-1545.2004.03.005

Synthetic Method and Surface-active Property of C8F17SO2N(C2H5)C2H4(OC2H4)nOH

  • C8F17SO2N(C2H5)C2H4(OC2H4)nOH surfactant is obtained from perfluorooctanesulfonyl fluoride through three-step reactions of amidation with ethylamine in the presence of isopropyl ether, reaction with 2-chlorohydrin, and then reaction with ethylene oxide in high temperature and high pressure. The surface-active property of the surfactant is investigated and the surface tension could reach below 19.2mN/m in 0.05%(wt) solution. IR,NMR,DSC and TG are employed to characterize the surfactant in this paper.
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