LIU Mei-ying, GUO Chuan-hua, DAN Nan-nan. Preparation of Nickel Sulfide Nanoparticles by Solvothermal Method[J]. Development and Application of Materials, 2010, 25(3): 61-65. DOI: 10.19515/j.cnki.1003-1545.2010.03.014
Citation: LIU Mei-ying, GUO Chuan-hua, DAN Nan-nan. Preparation of Nickel Sulfide Nanoparticles by Solvothermal Method[J]. Development and Application of Materials, 2010, 25(3): 61-65. DOI: 10.19515/j.cnki.1003-1545.2010.03.014
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Preparation of Nickel Sulfide Nanoparticles by Solvothermal Method

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  • Ni3S2, α-NiS and NiS2 nanocrystals were synthesized by the reaction of nickel nitrate and thiourea in ethylene glycol via a solvothermal process.The products were characterized by XRD and TEM.The results show that both the temperature and the molar ratio of nickel nitrate to thiourea put a significant effect on the phase and morphology of nickel sulfide powders.
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