Effect of Annealing Temperature on Microstructure and Mechanical Property of High Purity Titanium Cold Rolled Plate

CHANG Saipeng; WANG Bingxing; JIAO Jingjing; TIAN Yong; WANG Bin

Volume 39 Issue 4

Aug. 2024

Turn off MathJax

Article Contents

Abstract

References

Development and Application of Materials > 2024 > 39(4): 45-52.

CHANG Saipeng, WANG Bingxing, JIAO Jingjing, TIAN Yong, WANG Bin. Effect of Annealing Temperature on Microstructure and Mechanical Property of High Purity Titanium Cold Rolled Plate[J]. Development and Application of Materials, 2024, 39(4): 45-52.

Citation:

PDF (16803 KB)

Effect of Annealing Temperature on Microstructure and Mechanical Property of High Purity Titanium Cold Rolled Plate

State Key Laboratory of Rolling Technology and Continuous Rolling Automation, Northeastern University, Shenyang 110819, China

More Information

Received Date: March 04, 2024
Available Online: September 11, 2024

Graphical Abstract

Abstract

Abstract

The cold rolled high purity (99.995%) titanium plate with 60% reduction is annealed at different temperatures. The microstructure of the high-purity titanium plate is characterized by EBSD technology, and the tensile and hardness tests are carried out. The results show that with the increase of annealing temperature, the tensile strength and hardness of the high-purity titanium plate decrease continuously, and the elongation increases. After annealing at 600 ℃ for 10 minutes, the elongation of the plate reaches (74.6±5.0)%, and the tensile strength reaches (217±2) MPa. The microstructure shows that the grains have been completely transformed into equiaxed grains without distortion after being annealed at 600 ℃ for 10 minutes, and that the KAM value is reduced to 0.16°, indicating that there is almost no local strain and stored energy in the plate at this moment. The reason is that with the increase of annealing temperature, the dislocation density of the grain decreases, and the softening effect increases.
- high purity titanium,
- recrystallization nucleation,
- texture,
- mechanical property,
- KAM

FullText(HTML)

References (22)

References

[1]	GEETHA M, SINGH A K, ASOKAMANI R, et al. Ti based biomaterials, the ultimate choice for orthopaedic implants-a review[J]. Progress in Materials Science, 2009, 54(3):397-425.
[2]	NIINOMI M, NAKAI M, HIEDA J. Development of new metallic alloys for biomedical applications[J]. Acta Biomaterialia, 2012, 8(11):3888-3903.
[3]	KARIMI M, TOROGHINEJAD M R, DUTKIEWICZ J. Nanostructure formation during accumulative roll bonding of commercial purity titanium[J]. Materials Characterization, 2016, 122:98-103.
[4]	CHEN X, XIAO H, SHI Y M, et al. The influence of bonding time on microstructure and mechanical properties of vacuum diffusion bonded joints between commercial pure titanium and medium carbon steel[J]. Vacuum, 2023, 214:112158.
[5]	KLEVTSOV G V, VALIEV R Z, KLEVTSOVA N A, et al. Strength and fracture mechanism of an ultrafi-negrained austenitic steel for medical applications[J]. Materials, 2021, 14(24):7739.
[6]	KAZEMZADEH-NARBAT M, LAI B F, DING C F, et al. Multilayered coating on titanium for controlled release of antimicrobial peptides for the prevention of implant-associated infections[J]. Biomaterials, 2013, 34(24):5969-5977.
[7]	ISLAMGALIEV R K, KAZYHANOV V U, SHESTAKOVA L O, et al. Microstructure and mechanical properties of titanium (Grade 4) processed by high-pressure torsion[J]. Materials Science and Engineering:A, 2008, 493(1-2):190-194.
[8]	TERADA D, INOUE S, TSUJI N. Microstructure and mechanical properties of commercial purity titanium severely deformed by ARB process[J]. Journal of Materials Science, 2007, 42(5):1673-1681.
[9]	ZHANG F, FENG J, XIANG W, et al. Microstruc-ture evolution, grain refinement, and mechanical properties of a metastable β titanium alloy during cold rolling and recrystallization annealing[J]. Materials Characterization, 2024, 208:113632.
[10]	GU Y X, MA A B, JIANG J H, et al. Simultaneously improving mechanical properties and corrosion resistance of pure Ti by continuous ECAP plus short-duration annealing[J]. Materials Characterization, 2018, 138:38-47.
[11]	BRITTON T B, LIANG H, DUNNE F P E, et al. The effect of crystal orientation on the indentation response of commercially pure titanium:experiments and simulations[J]. Proceedings of the Royal Society A:Mathematical, Physical and Engineering Sciences, 2010, 466(2115):695-719.
[12]	郭庆,余伟,韩盈,等.压下率对冷轧及退火纯钛板材织构的影响[J].钛工业进展, 2022, 39(4):6-11.
[13]	张鹏飞.密排六方结构金属基面双峰织构的形成及演化机制研究[D].重庆:重庆大学, 2021.
[14]	毛卫民,赵新兵.金属的再结晶与晶粒长大[M].北京:冶金工业出版社, 1994.
[15]	赵鹏程.温度及应力诱发超细晶工业纯钛再结晶与晶粒长大的机理研究[D].上海:华东理工大学, 2020.
[16]	WU G C, LI S Y, LI J H, et al. Texture evolution during multi-pass cold rolling and annealing of Ti-2Al-1.5Mn alloy[J]. Journal of Alloys and Compounds, 2024, 971:172705.
[17]	ZHAO S, WANG Y, PENG L, et al. Effect of annealing temperature on microstructure and mechanical properties of cold-rolled commercially pure titanium sheets[J]. Transactions of Nonferrous Metals Society of China, 2022, 32(8):2587-2597.
[18]	WANG Y N, HUANG J C. Texture analysis in hexagonal materials[J]. Materials Chemistry and Physics, 2003, 81(1):11-26.
[19]	LUNT D, XU X, BUSOLO T, et al. Quantification of strain localisation in a bimodal two-phase titanium alloy[J]. Scripta Materialia, 2018, 145:45-49.
[20]	CHOI S W, LI C L, WON J W, et al. Deformation heterogeneity and its effect on recrystallization behavior in commercially pure titanium:comparative study on initial microstructures[J]. Materials Science and Engineering:A, 2019, 764:138211.
[21]	XU T F, WANG S Y, WANG W C, et al. Multimodal grain structure and tensile properties of cold-rolled titanium after short-duration annealing[J]. Materials Characterization, 2020, 160:110095.
[22]	ZHANG K, LIU X, FAN P, et al. Characterization of geometrically necessary dislocation evolution during creep of P91 steel using electron backscatter diffrac-tion[J]. Materials Characterization, 2023, 195.

[1]	HOU Lili, GUO Qiang, YAO Yuhong, LIU Jiangnan. Microstructure and Mechanical Properties of Annealed CoFeNiCrMnB_x High Entropy Alloy[J]. Development and Application of Materials, 2023, 38(2): 44-48.
[2]	WANG Yuan, DONG Jian, GUAN Yulong, ZHAO Baojie, ZHANG Haishen. Effect of Process on Microstructure and Mechanical Properties of TA5 Alloy Sheets[J]. Development and Application of Materials, 2022, 37(4): 61-64.
[3]	MA Weigang, ZHANG Youjing, YANG Chaofei, XUE Gang, WANG Renfu. Effect of Manganese Content on Microstructure and Mechanical Properties of Manganese Steel[J]. Development and Application of Materials, 2020, 35(3): 26-31.
[4]	HUANG Wei, WANG Shaogang, LI Lize, JIN Yang. Laser Beam Welding of Titanium Alloy and Microstructure and Mechanical Properties of Welded Joint[J]. Development and Application of Materials, 2019, 34(2): 20-27. DOI: 10.19515/j.cnki.1003-1545.2019.02.004
[5]	LIU Pengzheng, LI Dengfeng. Effect of AO-2246 on Damping and Mechanical Properties of Polyurethane[J]. Development and Application of Materials, 2019, 34(1): 88-92. DOI: 10.19515/j.cnki.1003-1545.2019.01.017
[6]	GAO Ling-qing, LI Hui, HOU Shi-zhong. Effects of Strain Rate and Temperature on the Mechanical Properties of 10NiCrMo Hull Steel[J]. Development and Application of Materials, 2013, 28(6): 9-14. DOI: 10.19515/j.cnki.1003-1545.2013.06.003
[7]	SUN Jian-gang, HU Wei-min, LIAO Zhi-qian, WANG Yang, ZHU Xiao-qing. Study on Texture and Mechanical Properties of the Ti6321 Titanium Alloy Sheet[J]. Development and Application of Materials, 2012, 27(2): 9-13. DOI: 10.19515/j.cnki.1003-1545.2012.02.003
[8]	GUAN Jian-dong, KANG Yong-lin, DU Xin, ZHENG Yue-qiang. Influence of Coiling Temperature and Total Cold Rolling Reduction Rate on Mechanical Properties of SPHD Steel[J]. Development and Application of Materials, 2009, 24(1): 39-42,46. DOI: 10.19515/j.cnki.1003-1545.2009.01.012
[9]	WANG Bing, SUN She-ying. An Investigation on the Influence of Molecular Structure upon Dynamic Mechanical Properties of Polymer Materials[J]. Development and Application of Materials, 2005, 20(3): 42-46. DOI: 10.19515/j.cnki.1003-1545.2005.03.013
[10]	Lou Guantao, Sun Jianke, Yang Xuedong, Chen Liping, Wang Bo, Chen Chunhe. Effects of Al and Mo on Mechanical Properties of Cast Titanium Alloys[J]. Development and Application of Materials, 2003, 18(4): 32-35. DOI: 10.19515/j.cnki.1003-1545.2003.04.010

Cited By

Get Citation

PDF

XML

Article Metrics

Article views (103) PDF downloads (36)

Effect of Annealing Temperature on Microstructure and Mechanical Property of High Purity Titanium Cold Rolled Plate

Abstract

References

Related Articles

Catalog

Article Metrics

Related

Effect of Annealing Temperature on Microstructure and Mechanical Property of High Purity Titanium Cold Rolled Plate

Abstract

References

Related Articles

Catalog

Article Metrics

Related

Export File

Citation

Format

Content