FAN Xuemei, WANG Shumin, LI Zhejian, WANG Yimeng, LIU Ping, FAN Xinhui. Synthesis and Electrochemical Luminescence Characterization of CdSe/ZnSe Quantum Dots[J]. Development and Application of Materials, 2021, 36(1): 29-33.
Citation: FAN Xuemei, WANG Shumin, LI Zhejian, WANG Yimeng, LIU Ping, FAN Xinhui. Synthesis and Electrochemical Luminescence Characterization of CdSe/ZnSe Quantum Dots[J]. Development and Application of Materials, 2021, 36(1): 29-33.

Synthesis and Electrochemical Luminescence Characterization of CdSe/ZnSe Quantum Dots

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  • Received Date: May 06, 2020
  • The core-shell CdSe/ZnSe quantum dots were synthesized by hydrothermal method based on the similar crystal structure and wider band gap of ZnSe semiconductor nanomaterial. The effect of reaction temperature, reaction time and molar ratio of Cd:Zn on the synthesis of quantum dots were investigated.Resultsshowed that when the temperature was between 70~160℃, the ZnSe shell was being coated on the CdSe core. When the reaction time was between 0~4 hours, the shell could be uniformly coated on the core. When the molar ratio of core to shell was 1:3, the electrochemical luminescence performance was the best, and its electrochemical luminescence intensity was 6 times higher than that of CdSe quantum dots.
  • [1]
    HUANG R F,LIU H X,GAI Q Q,et al.A facile and sensitive electrochemiluminescence biosensor for Hg2+ analysis based on a dual-function oligonucleotide probe[J].Biosensors and Bioelectronics,2015,71(15):194-199.
    [2]
    杨炳君.碲化镉量子点对原代肝、肾细胞及氧化应激蛋白质的毒性研究[D].济南:山东大学,2014.
    [3]
    鲁理平,许来慧,康天放,等.量子点CdS电化学发光传感器对DNA损伤研究[J].分析化学,2013,41(6),805-810.
    [4]
    张召香.基于胶束反向扫集的毛细管电泳量子点电化学发光研究[J].化学学报,2019,77(2):179-183.
    [5]
    LIU X,CHENG L X,LEI J P,et al.Dopamine detection based on its quenching effect on the anodic electrochemiluminescence of CdS quantum dots[J].Analyst,2008,133(9):1161-1163.
    [6]
    LIU X,GUO L,CHENG L X,et al.Determination of nitrite based on its quenching effect on anodic electrochemiluminescence of CdS quantum dots[J].Talanta,2006,78(3),690-694.
    [7]
    LI Q L,DING S N.Multicolor electrochemiluminescence of core-shell CdS@ZnS quantum dots based on the size effect.Science China Chemistry,2016,59(11):1-5.
    [8]
    LIU Q,HAN M,BAO J C,et al.CdSe quantum dots as labels for sensitive immunoassay of cancer biomarker proteins by electrogenerated chemiluminescence[J].Analyst,2011,136(24):5197-5203.
    [9]
    田利,赵越,齐艳娟.CdSe量子点修饰电极电化学发光法测定叶酸[J].分子科学学报,2017,33(4):342-346.
    [10]
    LIGHTCAP I V,KAMAT P V.Fortification of CdSe quantum dots with graphene oxide.excited state interactions and light energy conversion[J].Journal of the American Chemical Society,2012,134(16):7109-7116.
    [11]
    TAN L J,WAN A J,LI H L,et al.Biocompatible quantum dots-chitosan nanocomposites for fluorescence detection of nitric oxide[J].Materials Chemistry &Physics,2012,134(2-3):562-566.
    [12]
    PARK C,YOON T H.L-cysteine-induced photoluminescence enhancement of CdSe/ZnSe quantum dots in aqueous solution[J].Colloids Surf.B,2010,75(2):472-477.
    [13]
    TOPURIA T,MÖCK P,LEI Y,et al.Highly uniform (Cd,Mn,Zn) Se/(Zn,Mn) Se quantum dot array formation by means of thermal treatments[J].Applied Physics Letters,2003,82(21),3635-3637.
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