Volume 39 Issue 3
Jun.  2024
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GE Ning, FAN Hao, WANG Jiachen, SHAO Zongyi, LI Mingyang. Determination of Iron Content in Ferrotungsten Alloy Powder by ICP-AES[J]. Development and Application of Materials, 2024, 39(3): 66-71.
Citation: GE Ning, FAN Hao, WANG Jiachen, SHAO Zongyi, LI Mingyang. Determination of Iron Content in Ferrotungsten Alloy Powder by ICP-AES[J]. Development and Application of Materials, 2024, 39(3): 66-71.
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Determination of Iron Content in Ferrotungsten Alloy Powder by ICP-AES

  • 1. CNNC North Nuclear Fuel Components Co., Ltd., Baotou, Inner Mongolia 014035;

  • 2. Key Laboratory of Preparation Technology of Special Irradiation Components for Nuclear Reactors, Baotou, Inner Mongolia, 014035;

  • 3. CNNC Key Laboratory of New Materials Research and Application Development, Baotou, Inner Mongolia 014035;

  • 4. Key Laboratory of Nuclear Fuel Element Enterprises in Inner Mongolia Autonomous Region, Baotou, Inner Mongolia 014035

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  • Received Date: June 27, 2023
  • Available Online: July 22, 2024
    Graphical Abstract
    • Abstract
  • Tungsten-ferro alloy is a kind of tungsten-based cermet dispersed fuel matrix with good properties, and the content of Fe will directly affect the service characteristics of the alloy. In order to accurately detect the Fe content in the ferrotungsten alloy powders, ferrotungsten alloy powder weighing 0.1 g is dissolved with nitric acid and hydrofluoric acid, and the 5.5 mol/L nitric acid is used for capacity determination, which can completely dissolve the sample and effectively eliminate the influence of tungsten hydrolysis. The method for the determination of Fe content in the ferrotungsten powder by inductively coupled plasm-optical emission spectrometer (ICP-OES) has been developed. The experimental results show that the linear correlation coefficient intensity at 259.939 nm of Fe element can reach 0.999 985 when the instrument power is 1 300 W, the atomizer flow rate is 0.8 L/min, and the iron content in the sample is 1.5%-15.0%. The relative standard deviation (RSD) of the method can reach 0.45% (n=6), and the average recovery of the method is between 96% and 107%.
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    • References (6)
  • [1]
    中华人民共和国工业和信息化部.钨基高比重合金化学分析方法第2部分:铁、镍、铜含量的测定电感耦合等离子体原子发射光谱法:YS/T 1603.2-2023[S].北京:冶金工业出版社, 2023.
    [2]
    于文红. ICP-AES法测定钨合金中镍、钴、铁、锰时酸度的影响[J].光谱实验室, 1994, 11(2):52-56.
    [3]
    HLAVÁEK I, HLAVÁKOVÁ I. Multi-element analysis of ferrotungsten by inductively coupled plasma atomic emission spectrometry[J]. J Anal At Spectrom, 1986, 1(5):331-335.
    [4]
    成勇,彭慧仙,袁金红,等.微波消解-电感耦合等离子体原子发射光谱法测定钨基硬质合金中钴镍铁铌钽钒铬[J].冶金分析, 2013, 33(3):50-54.
    [5]
    石爱霞,刘百利.粉末压片-X射线荧光分析钽钛钨铁合金中钽钛钨铁[J].金属材料与冶金工程, 2009, 37(6):45-47.
    [6]
    黎福萍,钟映兰.钨铁合金中磷砷锡的联合测定[J].云南化工, 2021, 48(9):56-57.
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