Volume 37 Issue 6
Dec.  2022
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WANG Yaning, GAO Song, YANG Chunsheng. Application of Trace Elements Detection in Nickel-based Superalloys Based on Ammonia Coordination and Inductively Coupled Plasma Tandem Mass Spectrometry[J]. Development and Application of Materials, 2022, 37(6): 108-113.
Citation: WANG Yaning, GAO Song, YANG Chunsheng. Application of Trace Elements Detection in Nickel-based Superalloys Based on Ammonia Coordination and Inductively Coupled Plasma Tandem Mass Spectrometry[J]. Development and Application of Materials, 2022, 37(6): 108-113.
shu

Application of Trace Elements Detection in Nickel-based Superalloys Based on Ammonia Coordination and Inductively Coupled Plasma Tandem Mass Spectrometry

  • 1. AECC Beijing Institute of Aeronautical Materials, Beijing 100095, China;

  • 2. Beijing Key Laboratory of Aeronautical Materials Testing and Evaluation, Beijing 100095, China;

  • 3. Key Laboratory of Aeronautical Materials Testing and Evaluation Aero Engine Corporation of China, Beijing 100095, China

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  • Received Date: September 05, 2022
  • Available Online: January 11, 2023
    Graphical Abstract
    • Abstract
  • The detection method of various trace elements in nickel-based superalloys is developed based on the valence theory of NH3 coordination. Zn is taken as an example. With NH3 as the reaction gas, Zn reacts with NH3, and the product ion Zn(NH3)x can only be detected, which can eliminates the multi-atomic ion interference. Through determining the ion product and optimizing the velocity of the air flow and rejection parameter, the detection limit of Zn is as low as 0.13 μg/g with the standard deviation of 4.2%-5.1%, and the recovery rate is 93.0%-103.0%. The method processes low detection limit, high sensitivity, and high accuracy, and is hopeful to be applied to the detection of various trace elements (such as Ag, Cu, V, and Fe) in nickel-based superalloys.
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    • References (19)
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